104 14 158 3 1418 document 158 Supplementary Files for Chemical Characterizations of Isomeric Flavonoid Glycosides and Other Constituents from Ficus deltoidea Jack.zip application/zip 7acf5d484959f96b83c120cf81a0659a MD5 32989681 2024-03-19 07:16:37 http://data.uitm.edu.my/id/eprint/104/1/Supplementary%20Files%20for%20Chemical%20Characterizations%20of%20Isomeric%20Flavonoid%20Glycosides%20and%20Other%20Constituents%20from%20Ficus%20deltoidea%20Jack.zip 104 1 1 application/zip archive en public cc_by_nc_nd_4

Supplementary Files for Chemical Characterizations of Isomeric Flavonoid Glycosides and Other Constituents from Ficus deltoidea Jack.zip

published archive 2 disk0/00/00/01/04 2024-03-19 07:42:50 2025-04-15 13:47:22 2024-03-19 07:42:50 dataset show Afzan Adlin 0000-0001-9050-4648 Marcourt Laurence 0000-0002-9614-1099 Abd Karim Hidayatul Atiqah 0000-0003-1702-7149 Kasim Noraini 0000-0002-9692-2450 Ferreira Queiroz Emerson 0000-0001-9567-1664 Osman Che Puteh 0000-0002-9481-4050 Ismail Nor Hadiani 0000-0002-2374-4630 Wolfender Jean-Luc 0000-0002-0125-952X pub applied_sciences fsg Nuclear Magnetic Resonance, Natural Product, Liquid Chromatography Mass Spectrometry Steps to reproduce The 22 chemical constituents were purified using multiple chromatographic methods (e.g., high-speed counter-current chromatography, medium-pressure liquid chromatography, preparative and recycling high-performance liquid chromatography) from Ficus deltoidea leaves. All constituents were identified unambiguously based on spectroscopic data (NMR, UV and MS). NMR spectra were recorded on a 500 MHz Varian Inova spectrometer or CryoProbe Bruker 600 MHz spectrometer. The LC-PDA-MS were acquired using an Acquity UHPLC system coupled with a Micromass LCT Premier Time-of-Flight mass spectrometer (ToF-MS) and photodiode array (PDA) detector (Waters, Milford, USA). The presented NMR and LC-PDA-MS processed spectra are supplementary files for "Chemical characterizations of isomeric flavonoid glycosides and other constituents from Ficus deltoidea Jack". These datasets were analyzed to elucidate 22 chemical constituents identified as gallocatechin (S1), afzelechin-4-8"-gallocatechin (S2), catechin (S3), afzelechin-4-8"-catechin (S4), afzelechin (S5), epicatechin (S6), hovetrichoside C (S7), 6,8-di-C-D-glucopyranosylapigenin (vicenin-2) (S8), afzelechin-4-8"-epiafzelechin (S9), epiafzelechin (S10), 6-C-β-D-xylopyranosyl-8-C-β-D-glucopyranosylapigenin (vicenin-1) (S11), orientin (S13), schaftoside (S14), 6-C-D-glucopyranosyl-8-C-D-xylopyranosylapigenin (vicenin-3) (S16), vitexin (S17), vitexin 2"-O-rhamnoside (S19), isovitexin 2"-O-rhamnoside (S20), 6,8-di-C-α-L-arabinopyranosylapigenin (S21), 6,8-di-C-D-xylopyranosylapigenin (S22), 6-C-L-arabinopyranosyl-8-C-D-xylopyranosylapigenin (S23), rhoifolin (S24) and cerberic acid A (S26). The LC-PDA-MS files contained the base peak chromatogram, photodiode array chromatogram, MS spectra, calculated molecular formula and UV spectra. The NMR files consisted of the proton, carbon, APT, DEPTQ, HSQC, COSY, HMBC, ROESY and TOCSY NMR spectra. 2024-03-15 published https://data.mendeley.com/datasets/xgs4vs2b79/1 10.17632/xgs4vs2b79.1 public https://www.sciencedirect.com/science/article/pii/S2352340924003834 publication Ministry of Agriculture and Food Industries (Malaysia) 100-RMI/MOA 16/6/2 (2/2013 PDF medical_and_health_sciences